施設・装置 (NMR systems)

(1) 800 MHz ワイドボア固体高分解能NMRシステム(機構内利用のみ)

 800 MHz wide-bore solid-state NMR system: NIMS users only
 Manufacturers: Japan Superconductor Technology Inc.
        / JEOL RESONANCE Ltd.
 Spectrometer: JNM-ECZ800R
 Specifications:
 ・Magnetic field: 18.79 T (1H: 800 MHz)
 ・Room temperature bore: 89 mm
 ・Probes:
  HX (1 mmφ/70 kHz, 2 mmφ/40 kHz, 3.2 mmφ/22 kHz),
  Cryocoil (Optional)
 ・CP/MAS, MQMAS etc.
(2) 800 MHz ナローボア固体高分解能NMRシステム

 800 MHz narrow-bore solid-state NMR system
 Manufacturers: Japan Superconductor Technology Inc.
        / JEOL RESONANCE Ltd.
 Spectrometer: JNM-ECA 800
 Specifications:
 ・Magnetic field: 18.79 T (1H: 800 MHz)
 ・Room temperature bore: 54 mm
 ・Probes: HX (1 mmφ/70 kHz, 3.2 mmφ/22 kHz)
 ・CP/MAS, MQMAS, Low γ-MAS
(3) 500 MHz 固体高分解能NMRシステム

 500 MHz high-resolution solid-state NMR system
 Manufacturers: Japan Superconductor Technology Inc.
        / JEOL RESONANCE Ltd.
 Spectrometer: JNM-ECZ500R (Renewal, January 2021)
 Specifications:
 ・Magnetic field: 11.75 T (1H: 500 MHz)
 ・Room temperature bore: 89 mm
 ・Variable temperature unit (-150 ℃ ~ +250 ℃)
 ・Probes:
  HX (3.2 mmφ/22 kHz, 4 mmφ/15 kHz)
  HX (4 mmφ/15 kHz with a Low-γ kit, Phoenix)
  HXY (4 mmφ/15 kHz)
  Static (6 mmφ, with an optional goniometer, Doty)
 ・CP/MAS, MQMAS, Static (anisotropy)
 ・Remote Operation through WebEX system (NEW!)
(4) 500 MHz 固体汎用NMRシステム

 500 MHz multi-purpose solid-state NMR system
 Manufacturers: Oxford Instruments Plc.
        / JEOL RESONANCE Ltd.
 Spectrometer: JNM-ECA 500
 Specificataions:
 ・Magnetic field: 11.75 T (1H: 500 MHz)
 ・Room temperature bore: 89 mm
 ・Probes:
  HX (3.2 mmφ/22 kHz, 4 mmφ/15 kHz)
  HX (4 mmφ/15 kHz with a Low-γ kit, Phoenix)
  HXY (4 mmφ/15 kHz)
  Static (home-built, with a He gas-flow cryostat)
 ・CP/MAS, Static (broad line at cryotemperatures), etc.
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