Solid-State NMR
(The 2nd NMR Laboratory at Sakura)
- 500 MHz Solid-State NMR (Ⅰ)
This system is equipped with a superconducting magnet (11.75 T) and allows sample spinning up
to 22 kHz for high-resolution solid-state NMR. This allows broad-line NMR measurement.
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500 MHz superconducting magnet for high-resolution and solid-state NMR
Field: 11.75 tesla, 89 mm bore
Specifications
・Continuous operation in the persistent current mode (500 MHz)
・Magnetic field homogeneity: 2.6× 10
-6/ 20 mm DSV
・Room-temperature shim
・4 mm CPMAS, 3.2 mm CPMAS, and 4 mm HXYMAS
- 500 MHz Solid-State NMR (Ⅱ)
This system is equipped with a superconducting magnet (11.75 T) and allows sample spinning up
to 22 kHz for high-resolution solid-state NMR. The sample temperature can be continuously
Changed from -150 to +250℃
×
500 MHz superconducting magnet for high-resolution and solid-state NMR
Field: 11.75 tesla, 89 mm bore
Specifications
・Continuous operation in the persistent current mode (500 MHz)
・Magnetic field homogeneity: 2.6×10
-6/ 20 mm DSV
・Room-temperature shim
・4 mm CPMAS, 3.2 mm CPMAS, and 4 mm HXYMAS
- 800MHz solid-state high-resolution NMR
This system is equipped with a superconducting magnet (18.79 T) and allows sample
spinning up to 22 kHz for high-resolution solid-state NMR. This allows sample spinning up to
80 kHz using 1 mm CPMAS probe.
×
800 MHz superconducting magnet for high-resolution and solid-state NMR
Field: 18.79 tesla, 54 mm bore
Specifications
・Continuous operation in the persistent current mode (800 MHz)
・Magnetic field homogeneity: 2.6×10
-6/ 20 mm DSV
・Room-temperature shim
・3.2 mm CPMAS (
13C,
27Al, and
23Na), 3.2 mm MQMAS (from
207Pb to
87Sr),
and 1 mm CPMAS (
13C,
27Al, and
23Na)