Compound Cu4TiS4
Reaction
Phase transition
Cu4TiS4
Reagent
Rare Metallic Cu2S powder (3N 300mesh)
Ti(3N 100mesh)
S(6N)
Weight
100mg
Container
SiO2 glass ampoule
Comment
Phase transition of synthesized Cu4TiS4
Figure shows the first heating and cooling processes.(RT→800℃→RT)There exist four peaks.
On heating : at 651℃, 670℃, 704℃
On cooling:at 634℃
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