Compound Cu4TiS4
Reaction
Phase transition Cu4TiS4


ReagentRare Metallic Cu2S powder (3N 300mesh)

Ti(3N 100mesh)

S(6N) 
Weight100mg
ContainerSiO2 glass ampoule
Comment  Phase transition of synthesized Cu4TiS4
Figure shows the first heating and cooling processes.(RT→800℃→RT)There exist four peaks.
On heating : at 651℃, 670℃, 704℃
On cooling:at 634℃  
DSChome